
Instrument - Perkin-Elmer high temperature DTA7
Samples - solids (bulks, ribbons, powders) or viscous liquids of ~ 10 - 350 mg mass or up to 100 mm3
T, Temperature region, - from 25 oC up to 1500 oC.
w, Heating/cooling rate - from 0 up to 100 oC/min.
Atmosphere – dynamic argon, nitrogen, oxygen, air.
Investigated subjects, generally:
Thermodynamic stability of the samples.
Temperatures of the phase transformations (+/- 2 oC).
Heats of the phase transformations (+/- 4 J/g).
Kinetics of phase transformations in the samples.