DTA - (Differential thermal analysis)

 


Instrument - Perkin-Elmer high temperature DTA7

Samples - solids (bulks, ribbons, powders) or viscous liquids of ~ 10 - 350 mg mass or up to 100 mm

T, Temperature region, - from 25 oC up to 1500 oC. 

w, Heating/cooling rate - from 0 up to 100 oC/min.

Atmosphere – dynamic argon, nitrogen, oxygen, air.

 

Investigated subjects, generally:

Thermodynamic stability of the samples.

Temperatures of the phase transformations (+/- 2 oC).

Heats of the phase transformations (+/- 4 J/g).

Kinetics of phase transformations in the samples.

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